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ANALYSIS OF CRYSTAL STRUCTURE AND FUNCTIONAL GROUPS OF NiFe2O4 USING SOL GEL METHOD

Mashadi, Mashadi and Yunasfi, Yunasfi and Ari Adi, Wisnu (2016) ANALYSIS OF CRYSTAL STRUCTURE AND FUNCTIONAL GROUPS OF NiFe2O4 USING SOL GEL METHOD. Jurnal Sains Materi Indonesia, 17 (03). pp. 131-135. ISSN 1411-1098

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Abstract

A synthesis and characterization NiFe2O4 with sol gel method have been conducted. Fe2(NO3)3.9H2O powder mixed with Ni(NO3)2 was dissolved in 50 ml of polyethylene glycol at room temperature, then heated at a temperature of approximately 60 °C for 1 hour while stirring to form a wet gel. The gel was then dried in an oven at 120 °C for 5 hours and grinded to form a powder NiFe2O4. NiFe2O4 powder was then heated with a furnace at a temperature variation of 400°C, 600 °C, 800 °C and 1000 °C for 5 hours respectively. X-Ray Diffraction (XRD) pattern indicates that in this stage the sample is single phase. Fourier Transform Infra Red (FT-IR) spectroscopy analysis showed two absorption bands in the range of 411 and 599 cm-1 related to octahedral and tetrahedral sites. Kata Kunci : NiFe2O4, Sol gel, Crystal structure, Functional groups

Item Type: Article
Subjects: Daur Bahan Bakar Nuklir dan Bahan Maju > Bahan Struktur dan Bahan Maju > Teknik Sintesis Bahan Maju
Divisions: Pusat Sains dan Teknologi Bahan Maju
Depositing User: EDITOR PSTBM BATAN
Date Deposited: 03 May 2018 22:26
Last Modified: 19 May 2018 07:49
URI: http://repo-nkm.batan.go.id/id/eprint/772

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